Separation and Purification by Crystallization,9780841235137

Separation and Purification by Crystallization

by ; ;
ISBN13: 9780841235137
ISBN10: 0841235139
Format: Hardcover
Pub. Date: 1997-06-01
Publisher(s): Amer Chemical Society
List Price: $36.23

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Summary

Covering a range of topics, this volume presents crystallization of polymorphs and the problems encountered in the separation of chiral compounds by selective crystallization, as well as aspects of the crystallization of amino acids, proteins, and pharmaceuticals. The introductory section includes state-of-the-art research on secondary nucleation, the mechanism for crystallization of proteins, kinetics of impurity effect on growth, and crystal morphology prediction. Other topics include the use of high-pressure crystallization in industrial processes, precipitation cases for organic and inorganic compounds, precipitation processes by antisolvents, fast reaction precipitation, and isoelectric precipitation.

Table of Contents

Preface xi
BASIC STUDIES 2(44)
1. Crystal Morphology Predictive Techniques To Characterize Crystal Habit: Application to Aspirin (C(9)H(8)O(4))
2(16)
Paul Meenan
2. Mechanism of Crystal Growth of Protein: Differential Scanning Calorimetry of Thermolysin Crystal Suspension
18(10)
H. Ooshima
S. Urabe
K. Igarashi
M. Azuma
J. Kato
3. Source of Nuclei in Contact Nucleation as Revealed by Crystallization of Isomorphous Alums
28(8)
Manijeh M. Reyhani
Gordon M. Parkinson
4. A Kinetic Model for Unsteady-State Crystal Growth in the Presence of Impurity
36(10)
N. Kubota
M. Yokota
L.A. Guzman
CRYSTALLIZATION OF OPTICAL ISOMERS AND POLYMORPHS 46(90)
5. Concentration Change of L-SCMC [S-(Carboxymethyl)-L-cysteine] in a Supersaturated Solution of DL-SCMC with Suspended L-SCMC Seeds in a Batch Operation
46(13)
Ken Toyokura
M. Kurotani
J. Fujinawa
6. Purity Drop in Optical Resolution of Racemic Mixtures
59(14)
M. Matsuoka
7. Separation of L-Mandelic Acid from Asymmetric Mixtures by Means of High-Pressure Crystallization
73(10)
N. Nishiguchi
M. Moritoki
T. Shinohara
Ken Toyokura
8. Morphological Change Mechanism of Alpha-L-Glutamic Acid with Inclusion of L-Phenylalanine
83(9)
M. Kitamura
9. Growth Process and Morphological Change of Beta-Glutamic Acid in the Presence of L-Phenylalanine
92(9)
M. Kitamura
Y. Sumi
10. Crystallization Behaviors of Alpha- and Beta-Quizalofop-ethyl Polymorphs in Homogeneous Nucleation
101(10)
K. Miyake
O. Araki
M. Matsumura
11. Crystallization of Di-L-phenylalanine Sulfate Monohydrate from Fermentation Broth
111(12)
Tetsuya Kawakita
12. Characterization of Aluminum Trihydroxide Crystals Precipitated from Caustic Solutions
123(13)
Mei-yin Lee
Gordon M. Parkinson
Peter G. Smith
Frank J. Lincoln
Manijeh M. Reyhani
STUDIES RELATED TO INDUSTRIAL CRYSTALLIZERS AND PROCESSES 136(52)
13. Features of the High-Pressure Crystallization Process in Industrial Use
136(14)
M. Moritoki
N. Nishiguchi
S. Nishida
14. Semibatch Precipitation of a Metallized Dye Intermediate: Reaction and Precipitation Condition Effects on Particle Size and Filterability
150(22)
Kostas E. Saranteas
Gregory D. Botsaris
15. Effects of Seeding on Start-up Operation of a Continuous Crystallizer
172(16)
H. Takiyama
H. Yamauchi
M. Matsuoka
CRYSTALLIZATION OF PARTICULAR ORGANIC COMPOUNDS 188(42)
16. Recent Studies on Recovery of Oilseed Protein by Precipitation
188(22)
Matheo Raphael
Sohrab Rohani
Frank Sosulski
17. Secondary Crystallization of Paraffin Solidified on a Cooled Plane Surface
210(10)
K. Onoe
T. Shibano
S. Uji
Ken Toyokura
18. Crystallization of a Fatty Acid Mixture Using Spray Evaporation of Highly Volatile Solvents
220(10)
K. Maeda
H. Enomoto
K. Fukui
S. Hirota
CRYSTALLIZATION OF PARTICULAR INORGANIC COMPOUNDS 230(61)
19. Crystallization of Sodium Chloride with Amines as Antisolvents
230(12)
T.G. Zijlema
H. Oosterhof
G.J. Witkamp
G.M. van Rosmalen
20. Semibatch Gas Antisolvent Precipitation of Poly (2,6-dimethyl-1, 4-phenylene ether)
242(12)
F.E. Wubbolts
R.E.A. Buijsse
O.S.L. Bruinsma
J. de Graauw
G.M. van Rosmalen
21. Reactive Crystallization of Magnesium Hydroxide
254(13)
Hideki Tsuge
Kyoichi Okada
Toru Yano
Naoko Fukushi
Hiroko Akita
22. Phosphate Recovery by Reactive Crystallization of Magnesium Ammonium Phosphate: Application to Wastewater
267(10)
Izumi Hirasawa
Hiroyuki Nakagawa
Osamu Yosikawa
Masanori Itoh
23. Inclusion of Selenium in Ferrite Crystals
277(14)
Y. Taguchi
M. Ohizumi
K. Aoyama
K. Katoh
INDEXES 291
Author Index 291(1)
Affiliation Index 292(1)
Subject Index 292

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